1-Bromoadamantane Cas:768-90-1

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Product Description:

Product Name: 1-Bromoadamantane CAS NO:768-90-1

Synonyms:

1-Adamantyl Bromide;

Tricyclo[3.3.1.13,7]decane, 1-bromo-;

 

Chemical & Physical Properties:

Appearance : White to off-white powder.

Assay :≥99.0%

Density:1.448 g/cm3

Boiling Point:240.5℃ at 760 mmHg

Flash Point:96.4℃

Melting Point: 117-120℃

Water Solubility:It is soluble in organic solvents and insoluble in water.

 

Uses: It is an intermediate for the synthesis of amantadine hydrochloride.

Production method: derived from the bromination of adamantane. In a dry enamel glass pot, add adamantane, drop bromine, slowly increase the temperature to about 70 ℃, reflux for 6 hours. With the formation of 1-bromoadamantane, the reflux temperature of the reactants gradually increased, and finally reached 100°C. After the reaction, the temperature was left overnight. Then the temperature was raised to 45°C, and sodium bisulfite solution was added dropwise to remove excess bromine. Filter, wash the filter cake with water to neutral, and dry to obtain 1-bromoadamantane.

 

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Products under patent are offered for R & D purpose only. However, the final responsibility lies exclusively with the buyer.

 

 

 

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